MARC details
000 -LEADER |
fixed length control field |
02477cam a2200325 a 4500 |
003 - CONTROL NUMBER IDENTIFIER |
control field |
EG-GiCUC |
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
fixed length control field |
151125s2015 ua d f m 000 0 eng d |
040 ## - CATALOGING SOURCE |
Original cataloging agency |
EG-GiCUC |
Language of cataloging |
eng |
Transcribing agency |
EG-GiCUC |
041 0# - LANGUAGE CODE |
Language code of text/sound track or separate title |
eng |
049 ## - LOCAL HOLDINGS (OCLC) |
Holding library |
Deposite |
097 ## - Thesis Degree |
Thesis Level |
M.Sc |
099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC) |
Classification number |
Cai01.12.10.M.Sc.2015.Ah.S |
100 0# - MAIN ENTRY--PERSONAL NAME |
Personal name |
Ahmed Mohamed Abdelfattah Refaie Sultan |
245 10 - TITLE STATEMENT |
Title |
Synthesis and structure property relationship of some azo-ester organic compounds and their hydrogen-bonded complexes / |
Statement of responsibility, etc. |
Ahmed Mohamed Abdelfattah Refaie Sultan ; Supervised Abdelgawad Ali Fahmi , Magdi M. Naoum , Mohamed Ahmed Alaasar |
246 15 - VARYING FORM OF TITLE |
Title proper/short title |
تشييد وعلاقة التركيب بالخواص لبعض مركبات الأْزو-استر العضوية ومتراكبات الرابطة الهيدروجينية لها |
260 ## - PUBLICATION, DISTRIBUTION, ETC. |
Place of publication, distribution, etc. |
Cairo : |
Name of publisher, distributor, etc. |
Ahmed Mohamed Abdelfattah Refaie Sultan , |
Date of publication, distribution, etc. |
2015 |
300 ## - PHYSICAL DESCRIPTION |
Extent |
122 P. : |
Other physical details |
charts ; |
Dimensions |
25cm |
502 ## - DISSERTATION NOTE |
Dissertation note |
Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Organic Chemistry |
520 ## - SUMMARY, ETC. |
Summary, etc. |
Two series of new pyridine-based azo dyes were prepared. The first, namely 4-(3{u2032}-pyridylazophenyl)-4{u2032}{u2032}-alkoxy benzoates (In), is a homologous series that bears terminal alkoxy group with a number of carbon atoms varies between 8, 10, 12, 14, and 16 carbons, respectively. The terminal substituent, X, in the second series, Ia-e, is a compact group with certain polarity that, alternatively, changes between electron donating (CH3₃O, CH₃) and electron withdrawing (Br, NO₂), together with the unsubstituted one ( i.e., X= H). The structures of the prepared compounds were confirmed via infrared spectroscopy (IR), nuclear magnetic resonance (NMR), mass spectrometry and elemental analysis. Their mesophase behavior was investigated via differential scanning calorimetry (DSC) and polarized light microscopy (PLM). All homologues of the first series, (In), were found to be mesomorphic, while all derivatives of the latter, Ia-e, were nonmesomorphic |
530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE |
Additional physical form available note |
Issued also as CD |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
4-(3{u2032}-pyridylazophenyl)-4{u2032}{u2032}-alkoxy benzoates |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
4-substituted benzoic acids |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
Angular 1:1 hydrogen-bonded supramolecular liquid crystalline complexes |
700 0# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Abdelgawad Ali Fahmi , |
Relator term |
|
700 0# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Magdi M. Naoum , |
Relator term |
|
700 0# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Mohamed Ahmed Alaasar , |
Relator term |
|
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) |
Cataloger |
Aml |
Reviser |
Cataloger |
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) |
Cataloger |
Nazla |
Reviser |
Revisor |
942 ## - ADDED ENTRY ELEMENTS (KOHA) |
Source of classification or shelving scheme |
Dewey Decimal Classification |
Koha item type |
Thesis |