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Preparation and characterization of hematite / magnetite nanocomposites / (Record no. 58523)

MARC details
000 -LEADER
fixed length control field 02789cam a2200349 a 4500
003 - CONTROL NUMBER IDENTIFIER
control field EG-GiCUC
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20250223031610.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 161109s2016 ua dh f m 000 0 eng d
040 ## - CATALOGING SOURCE
Original cataloging agency EG-GiCUC
Language of cataloging eng
Transcribing agency EG-GiCUC
041 0# - LANGUAGE CODE
Language code of text/sound track or separate title eng
049 ## - LOCAL HOLDINGS (OCLC)
Holding library Deposite
097 ## - Thesis Degree
Thesis Level M.Sc
099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC)
Classification number Cai01.12.08.M.Sc.2016.Do.P
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Doaa Hanafi Mahmoud
245 10 - TITLE STATEMENT
Title Preparation and characterization of hematite / magnetite nanocomposites /
Statement of responsibility, etc. Doaa Hanafi Mahmoud ; Supervised Mohamed Abdelgawad Zayed , Mohamed Ali Ahmed , Neama Gomaa Imam
246 15 - VARYING FORM OF TITLE
Title proper/short title تحضير وتوصيف متراكبات نانوية للهيماتيت / والماجنيتيت
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Cairo :
Name of publisher, distributor, etc. Doaa Hanafi Mahmoud ,
Date of publication, distribution, etc. 2016
300 ## - PHYSICAL DESCRIPTION
Extent 176 P. :
Other physical details charts , facsimiles ;
Dimensions 25cm
502 ## - DISSERTATION NOTE
Dissertation note Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry
520 ## - SUMMARY, ETC.
Summary, etc. Herein, novel ferrofluid nanocomposites xFe₂O₃ {u200E}/ (1-x) Fe₂O₄ with different ratios (0.0 {u2264} x{u2264} 1.0) from magnetite and hematite nanoparticles (NPs); were prepared via sonochemical method, for the first time, for hyperthermia purposes. To confirm the correctness of these ratios chemical analyses of ferrous and ferric contents of the prepared nano composites were spectrophotometrically determined with and without indicators in the wavelength range 200-800 nm. Various analytical techniques have been used to analyze and characterize the crystalline structures of the prepared ferrofluid nanocomposites. X-ray diffraction (XRD) confirms the formation of two separate phases of nanocomposite components with average crystallite size ranges from 12-30 nm. The crystallite size was tuned via the hematite weight fraction x (wt %). FT-IR confirms the chemical composition of the two magnetic phases of the ferrofluid nanocomposites. The IR band at 627 cm⁻¹ is attributed to the Fe{u2013}O stretching vibrations and the band at 535cm⁻¹ is due to Fe{u2013}O in Fe₂O₃. High resolution transmission electron microscopy (HRTEM) and field emission scanning electron microscopy (FESEM) show the spherical and rod-like shape of magnetite and hematite respectively with average particle size of 12 nm for Fe₃O₄ NPs and 11 nm for Fe₂O₃ NPs. X-ray fluorescence (XRF) confirms that the nominal and chemical compositions are closed to each other. {u200E}
530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE
Additional physical form available note Issued also as CD
653 #4 - INDEX TERM--UNCONTROLLED
Uncontrolled term Hematite
653 #4 - INDEX TERM--UNCONTROLLED
Uncontrolled term Magnetite
653 #4 - INDEX TERM--UNCONTROLLED
Uncontrolled term Nanocomposites
700 0# - ADDED ENTRY--PERSONAL NAME
Personal name Mohamed Abdelgawad Zayed ,
Relator term
700 0# - ADDED ENTRY--PERSONAL NAME
Personal name Mohamed Ali Ahmed ,
Relator term
700 0# - ADDED ENTRY--PERSONAL NAME
Personal name Neama Gomaa Imam ,
Relator term
856 ## - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="http://172.23.153.220/th.pdf">http://172.23.153.220/th.pdf</a>
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN)
Cataloger Nazla
Reviser Revisor
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN)
Cataloger Soheir
Reviser Cataloger
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme Dewey Decimal Classification
Koha item type Thesis
Holdings
Source of classification or shelving scheme Not for loan Home library Current library Date acquired Full call number Barcode Date last seen Koha item type Copy number
Dewey Decimal Classification   المكتبة المركزبة الجديدة - جامعة القاهرة قاعة الرسائل الجامعية - الدور الاول 11.02.2024 Cai01.12.08.M.Sc.2016.Do.P 01010110070128000 22.09.2023 Thesis  
Dewey Decimal Classification   المكتبة المركزبة الجديدة - جامعة القاهرة مخـــزن الرســائل الجـــامعية - البدروم 11.02.2024 Cai01.12.08.M.Sc.2016.Do.P 01020110070128000 22.09.2023 CD - Rom 70128.CD