MARC details
000 -LEADER |
fixed length control field |
02096cam a2200313 a 4500 |
003 - CONTROL NUMBER IDENTIFIER |
control field |
EG-GiCUC |
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
fixed length control field |
170716s2016 ua f m 000 0 eng d |
040 ## - CATALOGING SOURCE |
Original cataloging agency |
EG-GiCUC |
Language of cataloging |
eng |
Transcribing agency |
EG-GiCUC |
041 0# - LANGUAGE CODE |
Language code of text/sound track or separate title |
eng |
049 ## - LOCAL HOLDINGS (OCLC) |
Holding library |
Deposite |
097 ## - Thesis Degree |
Thesis Level |
M.Sc |
099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC) |
Classification number |
Cai01.12.10.M.Sc.2016.Ne.S |
100 0# - MAIN ENTRY--PERSONAL NAME |
Personal name |
Nesma Abdellattif Abdelfattah |
245 10 - TITLE STATEMENT |
Title |
Synthesis of novel bis (heterocycles) of expected useful applications / |
Statement of responsibility, etc. |
Nesma Abdellattif Abdelfattah ; Supervsied Ahmed Helmy Elwhay , Ahmed Fathy Darweesh |
246 15 - VARYING FORM OF TITLE |
Title proper/short title |
تشييد حلقات غير متجانسة ثنائية متماثلة جديدة و متوقع لها تطبيقات مفيدة |
260 ## - PUBLICATION, DISTRIBUTION, ETC. |
Place of publication, distribution, etc. |
Cairo : |
Name of publisher, distributor, etc. |
Nesma Abdellattif Abdelfattah , |
Date of publication, distribution, etc. |
2016 |
300 ## - PHYSICAL DESCRIPTION |
Extent |
169 P. ; |
Dimensions |
25cm |
502 ## - DISSERTATION NOTE |
Dissertation note |
Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Organic Chemistry |
520 ## - SUMMARY, ETC. |
Summary, etc. |
Part 1: A novel series of bis-tetrahydro [1,2,4] triazolo [5,1-b] quinazolin-8 (4H)-ones were prepared via the three component reaction of bis-aldehydes with 3-amino-1,2,4-triazole and dimedone. The reaction mechanism was studied. Unambiguous structural elucidation of the regioisomers was done using DFT calculations as well as 2D-HMBC spectroscopy. Part 2: The synthetic utility of 2-thioxo-1,2-dihydropyridine-3-carbonitriles 3, 4 and 4-oxo-6-phenyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carbonitrile (19) as building blocks for novel bis-and poly(pyridines) as well as bis- and poly(pyrimidines) via alkylation with the corresponding bis-and poy(halo) compounds was investigated. Spectroscopic and theoretical studies confirmed the S-alkylation rather than the N-alkylation. The structures of all compounds are confirmed based on different spectral tools |
530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE |
Additional physical form available note |
Issued also as CD |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
Bis-aldehydes |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
Bis-tetrahydro [1,2,4] triazolo [5,1-b] quinazolin-8 4H-one |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
Multi-component reaction |
700 0# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Ahmed Fathy Darweesh , |
Relator term |
|
700 0# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Ahmed Helmy Elwhay , |
Relator term |
|
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) |
Cataloger |
Nazla |
Reviser |
Revisor |
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) |
Cataloger |
Samia |
Reviser |
Cataloger |
942 ## - ADDED ENTRY ELEMENTS (KOHA) |
Source of classification or shelving scheme |
Dewey Decimal Classification |
Koha item type |
Thesis |