Synthesis, characterization and photobiological activity of novel cephradine Schiff bases complexes / (Record no. 62479)
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| 000 -LEADER | |
|---|---|
| fixed length control field | 03242cam a2200349 a 4500 |
| 003 - CONTROL NUMBER IDENTIFIER | |
| control field | EG-GiCUC |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20250223031811.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 170924s2016 ua d f m 000 0 eng d |
| 040 ## - CATALOGING SOURCE | |
| Original cataloging agency | EG-GiCUC |
| Language of cataloging | eng |
| Transcribing agency | EG-GiCUC |
| 041 0# - LANGUAGE CODE | |
| Language code of text/sound track or separate title | eng |
| 049 ## - LOCAL HOLDINGS (OCLC) | |
| Holding library | Deposite |
| 097 ## - Thesis Degree | |
| Thesis Level | M.Sc |
| 099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC) | |
| Classification number | Cai01.24.05.M.Sc.2016.Ma.S |
| 100 0# - MAIN ENTRY--PERSONAL NAME | |
| Personal name | Marwa Mohammed Fathi Elnagdi |
| 245 10 - TITLE STATEMENT | |
| Title | Synthesis, characterization and photobiological activity of novel cephradine Schiff bases complexes / |
| Statement of responsibility, etc. | Marwa Mohammed Fathi Elnagdi ; Supervised Aida Lotfy Elansary , Tarek Abdallah Eltayeb , Nora S. Abdelkader |
| 246 15 - VARYING FORM OF TITLE | |
| Title proper/short title | تحضير و توصيف و دراسه النشاط البيولوجى الضوئى لمركبات قواعد شيف جديده مشتقه من السيفرادين |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. | |
| Place of publication, distribution, etc. | Cairo : |
| Name of publisher, distributor, etc. | Marwa Mohammed Fathi Elnagdi , |
| Date of publication, distribution, etc. | 2016 |
| 300 ## - PHYSICAL DESCRIPTION | |
| Extent | 115 P. : |
| Other physical details | charts ; |
| Dimensions | 25cm |
| 502 ## - DISSERTATION NOTE | |
| Dissertation note | Thesis (M.Sc.) - Cairo University - National Institute of Laser Enhanced Sciences - Department of Laser Application in Environmental Photochemistry and Agriculture |
| 520 ## - SUMMARY, ETC. | |
| Summary, etc. | A new Schiff bases L1 and L2 derived from the condensation of 6-formyl-7- hydroxy-5-methoxy-2-methylbenzopyran-4-one, derivative 1, (1) and 6-formyl-5,7- dihydroxy-2-methylbenzopyran-4-one, derivative 2, (2), respectively, with cephradine drug were prepared and characterized by elemental analyses and spectroscopic studies. Also, Zn(II), Cu(II), Co(II) and Ni(II) complexes of the schiff bases L1 and L2 were prepared by template reaction. Many tools of analysis such as elemental analyses, infrared, ultraviolet-visible and thermal analysis, as well as electrical conductance and magnetic susceptibility measurements were used to elucidate the structure of these complexes. The data showed that Zn(II)-L1 and Cu(II)-L1 complexes are 1:1 (M:L). The ligand L1was found to behave as monobasic bidentate in these complexes. On the other hand, Ni(II)-L1 and Co(II)-L1 form binuclear complexes. Ligand L2 acts as dibasic tetradentate in Zn(II)-L2, Cu(II)-L2, Ni(II)-L2 and Co(II)-L2 complexes which formed by stoichiometric ratio 2:1 (M:L). All the complexes are non-electrolytes. The luminescence properties of the prepared schiff bases and their complexes were studied. The photostability of Schiff bases and their Zn(II) and Cu(II) complexes were also studied. The photobiological activity of cephradine, benzopyran-4-one derivatives, L1, L2 Schiff bases and their complexes were studied on mosquito larvae to investigate the extent of their photosensitization efficiency in controlling noxious insects using direct sunlight(larvicidal effect). In vitro cytotoxicity study of the schiff base L1 and its complexes against HepG2 cell line was investigated by the MTT assay. The Schiff base, L1, exhibits better cytotoxic activity against HepG2 cell line than the complexes |
| 530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE | |
| Additional physical form available note | Issued also as CD |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Complexes |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Photostability |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Schiff bases |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Aida Lotfy Elansary , |
| Relator term | |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Nora S. Abdelkader , |
| Relator term | |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Tarek Abdallah Eltayeb , |
| Relator term | |
| 856 ## - ELECTRONIC LOCATION AND ACCESS | |
| Uniform Resource Identifier | <a href="http://172.23.153.220/th.pdf">http://172.23.153.220/th.pdf</a> |
| 905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) | |
| Cataloger | Nazla |
| Reviser | Revisor |
| 905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) | |
| Cataloger | Samia |
| Reviser | Cataloger |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Source of classification or shelving scheme | Dewey Decimal Classification |
| Koha item type | Thesis |
| Source of classification or shelving scheme | Not for loan | Home library | Current library | Date acquired | Full call number | Barcode | Date last seen | Koha item type | Copy number |
|---|---|---|---|---|---|---|---|---|---|
| Dewey Decimal Classification | المكتبة المركزبة الجديدة - جامعة القاهرة | قاعة الرسائل الجامعية - الدور الاول | 11.02.2024 | Cai01.24.05.M.Sc.2016.Ma.S | 01010110072754000 | 22.09.2023 | Thesis | ||
| Dewey Decimal Classification | المكتبة المركزبة الجديدة - جامعة القاهرة | مخـــزن الرســائل الجـــامعية - البدروم | 11.02.2024 | Cai01.24.05.M.Sc.2016.Ma.S | 01020110072754000 | 22.09.2023 | CD - Rom | 72754.CD |