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Development and modification of some pesticide residues analysis method in medicinal plants in Egypt and Morocco / (Record no. 66689)

MARC details
000 -LEADER
fixed length control field 02734cam a2200325 a 4500
003 - CONTROL NUMBER IDENTIFIER
control field EG-GiCUC
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 180708s2017 ua o f m 000 0 eng d
040 ## - CATALOGING SOURCE
Original cataloging agency EG-GiCUC
Language of cataloging eng
Transcribing agency EG-GiCUC
041 0# - LANGUAGE CODE
Language code of text/sound track or separate title eng
049 ## - LOCAL HOLDINGS (OCLC)
Holding library Deposite
097 ## - Thesis Degree
Thesis Level Ph.D
099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC)
Classification number Cai01.16.03.Ph.D.2017.Ha.D
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Hassan Abdelhalim Abdelfattah Elgammal
245 10 - TITLE STATEMENT
Title Development and modification of some pesticide residues analysis method in medicinal plants in Egypt and Morocco /
Statement of responsibility, etc. Hassan Abdelhalim Abdelfattah Elgammal ; Supervised Amira Shawky Soliman , Mohamed Said Abbas , Emad Ramadan Attallah
246 15 - VARYING FORM OF TITLE
Title proper/short title تطوير و تعديل طريقة تحليل بعض متبقيات المبيدات فى النباتات الطبية فى مصر و المغرب
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Cairo :
Name of publisher, distributor, etc. Hassan Abdelhalim Abdelfattah Elgammal ,
Date of publication, distribution, etc. 2017
300 ## - PHYSICAL DESCRIPTION
Extent 109 P. :
Other physical details photographs ;
Dimensions 25cm
502 ## - DISSERTATION NOTE
Dissertation note Thesis (Ph.D.) - Cairo University - Institute of African Research and Studies - Department of Natural Resources
520 ## - SUMMARY, ETC.
Summary, etc. Food safety is a high priority for human health. The multi-residue method of analysis for the determination of 323 pesticides in dry herbal products (chamomile and parsley) was developed as a target to improve products safety. The method has been optimized and validated using quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction method followed by liquid chromatography tandem mass spectrometry (LC-ESI-MS/MS) determination. The chosen pesticides belong to various chemical groups; they are registered in Egypt or most frequently detected in crops in the Egyptian market. The parameters of the triple quadrupole mass spectrometer (decluster potention and collesion energy) were optimized to gain maximum sensitivity. Method development was divided into three parts; extraction efficiency, clean up trails and matrix effect study. The extraction tests supported the use of a mechanical shaker in comparison with ultrasound and hand shaking. As a way to remove an interfering component from final extract, two different cleanup techniques were studied. Three matrix solid phase dispersion (C18, PSA, and GCB) were tested and evaluated. The obtained results showed limited number of pesticides covered. While the solid phase extraction (HLB) produced a good recovery with all substances without expecting reduction in matrix effect
530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE
Additional physical form available note Issued also as CD
653 #4 - INDEX TERM--UNCONTROLLED
Uncontrolled term LC-ESI-MS/MS
653 #4 - INDEX TERM--UNCONTROLLED
Uncontrolled term Medicinal plant
653 #4 - INDEX TERM--UNCONTROLLED
Uncontrolled term Pesticide residues
700 0# - ADDED ENTRY--PERSONAL NAME
Personal name Amira Shawky Soliman ,
Relator term
700 0# - ADDED ENTRY--PERSONAL NAME
Personal name Emad Ramadan Attallah ,
Relator term
700 0# - ADDED ENTRY--PERSONAL NAME
Personal name Mohamed Said Abbas ,
Relator term
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN)
Cataloger Nazla
Reviser Revisor
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN)
Cataloger Samia
Reviser Cataloger
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme Dewey Decimal Classification
Koha item type Thesis
Holdings
Source of classification or shelving scheme Not for loan Home library Current library Date acquired Full call number Barcode Date last seen Koha item type Copy number
Dewey Decimal Classification   المكتبة المركزبة الجديدة - جامعة القاهرة قاعة الرسائل الجامعية - الدور الاول 11.02.2024 Cai01.16.03.Ph.D.2017.Ha.D 01010110075292000 22.09.2023 Thesis  
Dewey Decimal Classification   المكتبة المركزبة الجديدة - جامعة القاهرة مخـــزن الرســائل الجـــامعية - البدروم 11.02.2024 Cai01.16.03.Ph.D.2017.Ha.D 01020110075292000 22.09.2023 CD - Rom 75292.CD