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Modified ion selective electrodes for potentiometric determination of clomipramine hydrochloride / Hager Mohammed Ibrahim Mohammed Tayea ; Supervised Mohamed M. A. Omar , Sally E. A. Elashery

By: Contributor(s): Material type: TextTextLanguage: English Publication details: Cairo : Hager Mohammed Ibrahim Mohammed Tayea , 2019Description: 103 P. : facsimiles ; 25cmOther title:
  • أقطاب أيونية إنتقائية معدلة للتقدير الجهدى لهيدروكلوريد الكلوميبرامين [Added title page title]
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  • Issued also as CD
Dissertation note: Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry Summary: In this work, clay-polyaniline polyfiber nanocomposite (MT-PANI{u2013}NF) was developed by chemical oxidative polymerization method and used for modification of three carbon paste electrodes as an electroactive material in absence or presence of graphene content to determine clomipramine hydrochloride (CLO-HCl) in pure form and pharmaceutical preparation. The electrodes were characterized and investigated with respect to the experimental parameters affecting their performance including temperature, pH, response time and interference. The electrodes showed good selectivity to CLO-HCl with respect to the interfering ions and inorganic cations. Determination of clomipramine hydrochloride in both pure and pharmaceutical form were performed using calibration and standard addition methods. Validation parameters such as accuracy, precision, linearity, specificity, limit of detection and limit of quantification were achieved. The obtained results were in a good agreement with those obtained by the reported method
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Item type Current library Home library Call number Copy number Status Date due Barcode
Thesis Thesis قاعة الرسائل الجامعية - الدور الاول المكتبة المركزبة الجديدة - جامعة القاهرة Cai01.12.08.M.Sc.2019.Ha.M (Browse shelf(Opens below)) Not for loan 01010110079943000
CD - Rom CD - Rom مخـــزن الرســائل الجـــامعية - البدروم المكتبة المركزبة الجديدة - جامعة القاهرة Cai01.12.08.M.Sc.2019.Ha.M (Browse shelf(Opens below)) 79943.CD Not for loan 01020110079943000

Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry

In this work, clay-polyaniline polyfiber nanocomposite (MT-PANI{u2013}NF) was developed by chemical oxidative polymerization method and used for modification of three carbon paste electrodes as an electroactive material in absence or presence of graphene content to determine clomipramine hydrochloride (CLO-HCl) in pure form and pharmaceutical preparation. The electrodes were characterized and investigated with respect to the experimental parameters affecting their performance including temperature, pH, response time and interference. The electrodes showed good selectivity to CLO-HCl with respect to the interfering ions and inorganic cations. Determination of clomipramine hydrochloride in both pure and pharmaceutical form were performed using calibration and standard addition methods. Validation parameters such as accuracy, precision, linearity, specificity, limit of detection and limit of quantification were achieved. The obtained results were in a good agreement with those obtained by the reported method

Issued also as CD

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