Eman Adel Hassan Rend

Production and evaluation of caffeine certified reference materials for its assessment in milk chocolate and coffee / إنتاج وتقييم مواد مرجعية للكافيين لإستخدامها فى تقييم شيكولاتة الحليب والقهوة Eman Adel Hassan Rend ; Supervised Mahmoud Sabry Mohamed Rizk , Adel Bassiouny Elsayed Shehata - Cairo : Eman Adel Hassan Rend , 2015 - 109 P. : charts ; 25cm

Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical chemistry

Reference materials are important tool in chemical analysis in terms of provision of traceability of the measurement results to the SI units. A Pure substance certified reference material from caffeine and matrix certified reference material of milk chocolate were developed for the content of caffeine and theobromine, theophylline and caffeine respectively. Homogeneity and stability of the prepared reference materials were studied and characterization was done by two independent analytical methods. The measurement results were statistically treated and the certified values of caffeine is 99.862 %±0.649 in pure substance certified reference material (caffeine) and they were 1393.2± 21.569, 0.499 ±0.054 and 112.48±3.897 mg/kg for theobromine, theophylline and caffeine in milk chocolate certified reference material which makes the candidate reference materials very useful as a calibrant and for quality achievement in chemical analysis




Referenc material and Homogeneity Study

Caffeine Milk chocolate