000 03430cam a2200349 a 4500
003 EG-GiCUC
005 20250223031721.0
008 170507s2016 ua dh f m 000 0 eng d
040 _aEG-GiCUC
_beng
_cEG-GiCUC
041 0 _aeng
049 _aDeposite
097 _aPh.D
099 _aCai01.09.10.Ph.D.2016.Ta.E
100 0 _aTamer Mohamed Hamdy Mahmoud Ibrahim
245 1 0 _aEffect of impregnation of calcium phosphate based nanofillers on acrylic bone cement :
_bIn vitro study /
_cTamer Mohamed Hamdy Mahmoud Ibrahim ; Supervised Sayed Hussein Sayed Saniour , Marwa Adel Elsayed Hammed , Rania Ahmad Helmy Salama
246 1 5 _aتأثير إشراب لاصق العظم الراتينجي بالمالئات النانومترية المعتمِدة على فوسفات الكالسيوم :
_bدراسة مخبرية
260 _aCairo :
_bTamer Mohamed Hamdy Mahmoud Ibrahim ,
_c2016
300 _a99 P. :
_bcharts , facsimiles ;
_c25cm
502 _aThesis (Ph.D.) - Cairo University - Faculty of Oral and Dental Medicine - Department of Dental Materials
520 _aCalcium phosphate (CaP) fillers were prepared by the sol-gel method. Characterization was done by means of X-ray diffraction (XRD) analysis and Fourier transform infrared spectroscopy (FTIR). Surface morphology, microstructure and particle size of the prepared particles was assessed by scanning and Transmission electron microscopy (SEM and TEM). In addition, decomposition and stability of the prepared CaP was analyzed by Differential scanning calorimetry (DSC)/Thermal gravimetric analysis (TGA). The change in pH after CaP dissolution in physiologic fluid was measured by pH-meter for 1, 3, 7 and 14 days and was extended for 7 more successive days after fixation of the pH value. Manual blending of the prepared nano filler; 0 weight %, 20 weight % and 40 weight % concentrations, into commercially available PMMA bone cement was done to prepare the polymer/nHA composite in an attempt to be used as bioactive bone cement. A total of 45 specimens (5 specimens per group) were then tested for the calcium and phosphorus ion release using inductively coupled plasma (ICP), hydroxyapatite crystals formation analyzed by energy dispersive x-ray spectroscopy (EDX) and compressive strength using universal testing machine.Results: Results of characterization of the prepared CaP confirmed preparation of a high purity amorphous nHA powder with uniform, rod-like, smooth surface particle, homogenously distributed particles with a size range of 3-10 nm and a very little degree of agglomeration. The prepared nHA powder showed thermal stability up to temperature of 200 {u00B0}C. Moreover, the pH changes of 5% CaP Tris-buffer solution over time was (7.59) which lied within physiological limits (6.5 to 7.8). ICP results revealed that 40 weight % filler specimens had the highest statistically significant calcium and phosphorus ion release values compared to 20 weight % filler and control specimens (0 weight % filler)
530 _aIssued also as CD
653 4 _aCalcium phosphate
653 4 _aCaP
653 4 _aHydroxyapatite
700 0 _aMarwa Adel Elsayed Hammed ,
_eSupervisor
700 0 _aRania Ahmad Helmy Salama ,
_eSupervisor
700 0 _aSayed Hussein Sayed Saniour ,
_eSupervisor
856 _uhttp://172.23.153.220/th.pdf
905 _aEnas
_eCataloger
905 _aNazla
_eRevisor
942 _2ddc
_cTH
999 _c60821
_d60821