000 02567cam a2200337 a 4500
003 EG-GiCUC
005 20250223032132.0
008 181212s2017 ua d f m 000 0 eng d
040 _aEG-GiCUC
_beng
_cEG-GiCUC
041 0 _aeng
049 _aDeposite
097 _aM.Sc
099 _aCai01.12.09.M.Sc.2017.Mo.M
100 0 _aMohamed Shawky Abdelfattah
245 1 0 _aMetal complexes of some new azo compounds derived from 4-aminoantipyrine :
_bpreparation, characterization and evaluation of their biological activity /
_cMohamed Shawky Abdelfattah ; Supervised Gehad Genidy Mohamed , Walaa Hamed Mahmoud
246 1 5 _aمتراكبات بعض مركبات الازو الجديدة المشتقه من 4- أمينونتيبيرينز:
_bتحضير وتوصيف وتقييم النشاط البيولوجي
260 _aCairo :
_bMohamed Shawky Abdelfattah ,
_c2017
300 _a133 P. :
_bcharts ;
_c25cm
502 _aThesis (M.Sc.) - Cairo University - Faculty of Science - Department of Inorganic Chemistry
520 _aThis work had been carried out to investigate the coordination behaviors of two newly synthesized azo dyes with different coordination sites, towards some bi- and trivalent metal ions like Cr(III), Mn(II), Fe(III), Co(II), Ni(II), Cu(II), Zn(II) and Cd(II). The two azo dye ligands and their solid chelates were prepared and subjected to many analytical techniques such as elemental analyses, mass spectroscopy, IR, ¹H NMR and solid reflectance spectra, magnetic moment, molar conductance, and thermal analyses techniques. The chelates were found to have an octahedral geometry. The two ligands and their metal complexes were subjected to thermal analyses (TG and DTG) and decomposition steps were demonstrated from their corresponding DTG curves to throw more light on the nature of changes accompanying the thermal decomposition process of these complexes. The antifungal activity (Aspergillus fumigatus and Candida albicans) and antibacterial activity against Gram positive (Staphylococcus aureus and Bacillus subtilis) and Gram negative (Salmonella sp and Escherichia coli) of the newly synthesized azo dye ligands and their metal complexes were also screened
530 _aIssued also as CD
653 4 _aAzo dye
653 4 _aElemental analyses
653 4 _aThermal analyses
700 0 _aGehad Genidy Mohamed ,
_eSupervisor
700 0 _aWalaa Hamed Mahmoud ,
_eSupervisor
856 _uhttp://172.23.153.220/th.pdf
905 _aNazla
_eRevisor
905 _aShimaa
_eCataloger
942 _2ddc
_cTH
999 _c69052
_d69052