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040 _aEG-GiCUC
_beng
_cEG-GiCUC
041 0 _aeng
049 _aDeposite
097 _aM.Sc
099 _aCai01.13.04.M.Sc.2019.Sa.F
100 0 _aSalma Tarek Abdelwahab Abdelazeem
245 1 0 _aFactors affecting the preparation of aluminum fluoride by the wet process from fluosilicic acid produced from phosphate fertilizers industry /
_cSalma Tarek Abdelwahab Abdelazeem ; Supervised Magdi Fouad Abadir , Ibrahim Ahmed Ibrahim
246 1 5 _aالعوامل المؤثرة على تحضير فلوريدالألومنيوم بالطريقة الرطبة من حمض الفلوسيلسيك الناتج عن صناعة الأسمدة الفوسفاتية
260 _aCairo :
_bSalma Tarek Abdelwahab Abdelazeem ,
_c2019
300 _a72 P. :
_bcharts , facsimiles ;
_c30cm
502 _aThesis (M.Sc.) - Cairo University - Faculty of Engineering - Department of Chemical Engineering
520 _aThis thesis deals with studying some of the factors affecting the preparation of anhydrous aluminum fluoride fit for several uses by the wet process. Different parameters were optimized along the preparation scheme, namely; kaolin particle size, acid concentration, temperature, reaction time and kaolin to acid ratio. Leaching reaction kinetics was studied using the isothermal technique and two models were found to best fit the obtained data, namely, the unreacted core model (diffusion through product layer controlled) and the progressive reaction model. Filtration process was performed under constant pressure using both vacuum and pressure filtration whereby the specific cake and filter medium resistances were obtained. Crystallization process was performed using the evaporative method with optimization of time and seeds type. Finally, the calcination step was carried out to obtain the final anhydrous product with purity more than 98%
530 _aIssued also as CD
653 4 _aAluminum fluoride
653 4 _aFluosilicic acid
653 4 _aPhosphate fertilizers industry
700 0 _aIbrahim Ahmed Ibrahim ,
_eSupervisor
700 0 _aMagdi Fouad Abadir ,
_eSupervisor
905 _aNazla
_eRevisor
905 _aShimaa
_eCataloger
942 _2ddc
_cTH
999 _c72539
_d72539