000 | 02219cam a2200313 a 4500 | ||
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003 | EG-GiCUC | ||
008 | 210823s2021 ua dh f m 000 0 eng d | ||
040 |
_aEG-GiCUC _beng _cEG-GiCUC |
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041 | 0 | _aeng | |
049 | _aDeposite | ||
097 | _aM.Sc | ||
099 | _aCai01.12.08.M.Sc.2021.He.D | ||
100 | 0 | _aHeba Aly Mohammad Marzouk | |
245 | 1 | 0 |
_aDetermination of some metal ions using carbon paste electrodes / _cHeba Aly Mohammad Marzouk ; Supervised Eman Yossri Frag , Marwa Elbadry Mohamed |
246 | 1 | 5 | _aتتقدير بعض أيونات العناصر بإستخدام أقطاب عجينة الكربون |
260 |
_aCairo : _bHeba Aly Mohammad Marzouk , _c2021 |
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300 |
_a72 P. : _bcharts , facimiles ; _c25cm |
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502 | _aThesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry | ||
520 | _aIn this paper, an effective, selective, and inexpensive Cr(III) ions modified carbon paste electrode (MCPE) based on benazepril (BNZ) was developed and described. It shows a good Nernstian slope of 19.20 + 0.39 mV decade-1 over a wide linear range of 8.0 {u00D7} 10-6{u2013} 1.0 {u00D7} 10-1 mol L-1 with a fast response time (10 s) and can be applied for measurements for at least 54 days with negligible change in results. The proposed sensor was pH-Independent in the range of 2.5{u2013}6.5 and showed an excellent selectivity towards Cr(III) ions over many other cations. The Cr(III)-BNZ surface interaction was investigated by using the energy dispersive X-ray analysis (EDX) and a scanning electron microscope (SEM). The proposed MCPE was completely validated according to the EURACHEM guidelines. Lastly, the proposed electrode efficiency for trace amount determination of Cr(III) ions in various food samples was examined, and the obtained results were compared with the results of the inductively coupled plasma-optical emission spectroscopy (ICP-OES) | ||
530 | _aIssued also as CD | ||
653 | 4 | _aChromium | |
653 | 4 | _aModified CPE | |
653 | 4 | _aSensor | |
700 | 0 |
_aEman Yossri Frag , _eSupervisor |
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700 | 0 |
_aMarwa Elbadry Mohamed , _eSupervisor |
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905 |
_aNazla _eRevisor |
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905 |
_aShimaa _eCataloger |
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942 |
_2ddc _cTH |
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999 |
_c81829 _d81829 |