Utility of enamines as precursors for Synthesis of new heterocycles / (Record no. 58263)
[ view plain ]
| 000 -LEADER | |
|---|---|
| fixed length control field | 02898cam a2200337 a 4500 |
| 003 - CONTROL NUMBER IDENTIFIER | |
| control field | EG-GiCUC |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20250223031602.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 161023s2016 ua d f m 000 0 eng d |
| 040 ## - CATALOGING SOURCE | |
| Original cataloging agency | EG-GiCUC |
| Language of cataloging | eng |
| Transcribing agency | EG-GiCUC |
| 041 0# - LANGUAGE CODE | |
| Language code of text/sound track or separate title | eng |
| 049 ## - LOCAL HOLDINGS (OCLC) | |
| Holding library | Deposite |
| 097 ## - Thesis Degree | |
| Thesis Level | M.Sc |
| 099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC) | |
| Classification number | Cai01.12.10.M.Sc.2016.Do.U |
| 100 0# - MAIN ENTRY--PERSONAL NAME | |
| Personal name | Doaa Mohamed Abdelmoniem Hassan |
| 245 10 - TITLE STATEMENT | |
| Title | Utility of enamines as precursors for Synthesis of new heterocycles / |
| Statement of responsibility, etc. | Doaa Mohamed Abdelmoniem Hassan ; Supervised Said Ahmed Soliman Ghozlan , Ismail Abdelshafy Abdelhamid |
| 246 15 - VARYING FORM OF TITLE | |
| Title proper/short title | استخدام الاينامينات كبادئات اولية لتحضير حلقات غير متجانسة الحلقة جديدة |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. | |
| Place of publication, distribution, etc. | Cairo : |
| Name of publisher, distributor, etc. | Doaa Mohamed Abdelmoniem Hassan , |
| Date of publication, distribution, etc. | 2016 |
| 300 ## - PHYSICAL DESCRIPTION | |
| Extent | 89 P. : |
| Other physical details | charts ; |
| Dimensions | 25cm |
| 502 ## - DISSERTATION NOTE | |
| Dissertation note | Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Organic Chemistry |
| 520 ## - SUMMARY, ETC. | |
| Summary, etc. | The original work of this thesis is composed of three parts. In the first part, a series of N-((1,2,4-triazol-3-yl)-enamine and N-((1,2,3-triazol-4-yl)-enamine were prepared and reacted with Ü,Ý-unsaturated nitriles to yield novel N-(4H-1,2,4-triazol-3-yl)- hexahydroquinoline-3-carbonitrile and their fused and spiro derivatives. Dimroth type rearrangement of the prepared quinoline derivatives was observed in acetic anhydride leading to the formation of substituted pyrimido[4,5-b]quinoline, spiro[indoline-3,5'-pyrimido[4,5- b]quinoline] and spiro[indoline-3,5'-[1,3]oxazino[4,5-b]quinoline] compounds. The second part, A simple and efficient one-pot synthesis of novel thieno[3',2':5,6]pyrimido[1,2- a]quinoline-2-carboxylates and their spirooxindole derivatives were accomplished via the Michael addition reaction of a cyclic Ý-enaminone incorporating thiophene moiety with Ü,Ý- unsaturated nitrile derivatives in EtOH at reflux in the presence of piperidine. Also, novel spirocyclic 2-oxoindole derivatives of thieno[3',2':5,6]pyrimido[1,2-a]quinolone were synthesized by the reaction this cyclic Ý-enaminone with 3-cyanomethylidene 2-oxoindole derivatives in refluxing EtOH. In the third part, The three-component reaction of dimedone, malononitrile dimer and bis-aldehydes in ethanol at reflux in the presence of piperidine afforded bis(5H-chromeno[2,3-b]pyridine-3-carbonitrile) derivatives in excellent yields. The chemical structures of all new synthesized products were confirmed based on the different spectral tools and elemental analysis data |
| 530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE | |
| Additional physical form available note | Issued also as CD |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Hexahydroquinoline |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Michael addition |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Ý-Enaminone |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Ismail Abdelshafy Abdelhamid , |
| Relator term | |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Said Ahmed Soliman Ghozlan , |
| Relator term | |
| 856 ## - ELECTRONIC LOCATION AND ACCESS | |
| Uniform Resource Identifier | <a href="http://172.23.153.220/th.pdf">http://172.23.153.220/th.pdf</a> |
| 905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) | |
| Cataloger | Nazla |
| Reviser | Revisor |
| 905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) | |
| Cataloger | Soheir |
| Reviser | Cataloger |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Source of classification or shelving scheme | Dewey Decimal Classification |
| Koha item type | Thesis |
| Source of classification or shelving scheme | Not for loan | Home library | Current library | Date acquired | Full call number | Barcode | Date last seen | Koha item type | Copy number |
|---|---|---|---|---|---|---|---|---|---|
| Dewey Decimal Classification | المكتبة المركزبة الجديدة - جامعة القاهرة | قاعة الرسائل الجامعية - الدور الاول | 11.02.2024 | Cai01.12.10.M.Sc.2016.Do.U | 01010110069860000 | 22.09.2023 | Thesis | ||
| Dewey Decimal Classification | المكتبة المركزبة الجديدة - جامعة القاهرة | مخـــزن الرســائل الجـــامعية - البدروم | 11.02.2024 | Cai01.12.10.M.Sc.2016.Do.U | 01020110069860000 | 22.09.2023 | CD - Rom | 69860.CD |