Applications of near infrared in pharmaceutical analysis / (Record no. 66996)
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| 000 -LEADER | |
|---|---|
| fixed length control field | 03312cam a2200349 a 4500 |
| 003 - CONTROL NUMBER IDENTIFIER | |
| control field | EG-GiCUC |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20250223032029.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 180808s2018 ua dh f m 000 0 eng d |
| 040 ## - CATALOGING SOURCE | |
| Original cataloging agency | EG-GiCUC |
| Language of cataloging | eng |
| Transcribing agency | EG-GiCUC |
| 041 0# - LANGUAGE CODE | |
| Language code of text/sound track or separate title | eng |
| 049 ## - LOCAL HOLDINGS (OCLC) | |
| Holding library | Deposite |
| 097 ## - Thesis Degree | |
| Thesis Level | Ph.D |
| 099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC) | |
| Classification number | Cai01.08.03.Ph.D.2018.Ah.A |
| 100 0# - MAIN ENTRY--PERSONAL NAME | |
| Personal name | Ahmed Shawky Abdalbakey Attia Abouzaid |
| 245 10 - TITLE STATEMENT | |
| Title | Applications of near infrared in pharmaceutical analysis / |
| Statement of responsibility, etc. | Ahmed Shawky Abdalbakey Attia Abouzaid ; Supervised Ahmed Emad Elgindy , Maissa Y. Salem , Eman Saad Elzanfaly |
| 246 15 - VARYING FORM OF TITLE | |
| Title proper/short title | {uFE97}{uFEC4}{uFE92}{uFBFF}{uFED8}{uFE8E}{uFE95} ا{uئإئ٧}{uئإآ٧}{uئإأأ}{uئإ٩٤} {uئإ٩٧}{uئإء٤}{uئإ٩٦} ا{uئإؤئ}{uئإء٤}{uئإإ٤}{uئإءإ}اء ا{uئإؤئ}{uئإؤ٨}{uئإءإ}{uئإئ٣}{uئإ٩٢}{uئإ٩٤} فى ا{uئإؤئ}{uئإ٩٨}{uئإء٤}{uئإإ٠}{uئآئئ}{uئإؤإ} ا{uئإؤئ}{uئإآأ}{uئآئئ}دلى |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. | |
| Place of publication, distribution, etc. | Cairo : |
| Name of publisher, distributor, etc. | Ahmed Shawky Abdalbakey Attia Abouzaid , |
| Date of publication, distribution, etc. | 2018 |
| 300 ## - PHYSICAL DESCRIPTION | |
| Extent | 258 P. : |
| Other physical details | charts , facsimiles ; |
| Dimensions | 25cm |
| 502 ## - DISSERTATION NOTE | |
| Dissertation note | Thesis (Ph.D.) - Cairo University - Faculty of Pharmacy - Department of Analytical Chemistry |
| 520 ## - SUMMARY, ETC. | |
| Summary, etc. | This thesis consists of four parts. Part (I): which includes an introduction to near infrared spectroscopy, raman spectroscopy, chemometrics, analytical method validation, process analytical technology and quality by design. Part (II): This part provides a general introduction about topical gel, chemical structure and physical properties of the ketoprofen, and the literature review of the applications of NIR spectroscopy and raman spectroscopy in pharmaceutical gel analysis. Three spectroscopic techniques; NIR transflection, NIR transmission and raman spectroscopy were developed and validated for determination of ketoprofen; the active ingredient in pharmaceutical topical gel.. The performance of the proposed methods was compared to determine the one with better performance. Part (III): This part provides a general introduction about granulation, fluid bed granulation (FBG), variables in FBG, plackett-burman design as an experimental design for screening purpose and the literature review of the applications of NIR spectroscopy in FBG end-point detection. Plackett-Burman design was used for screening the process variables in FBG and studies their influence on the pharmaceutical properties of the acetaminophen granules. Besides, both in-line (real-time) and at-line NIR reflectance methodologies were developed and validated for predictions of granule moisture content and granule size during the entire granulation process. Part (IV): Applications of NIR spectroscopy as a process analytical technology in tablet process development - blending uniformity of ibuprofen powder, and content uniformity, tablet hardness of ibuprofen tablet and dissolution profile of acetaminophen tablets |
| 530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE | |
| Additional physical form available note | Issued also as CD |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Granules |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Near infrared |
| 653 #4 - INDEX TERM--UNCONTROLLED | |
| Uncontrolled term | Process analytical technology |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Ahmed Emad Elgindy , |
| Relator term | |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Eman Saad Elzanfaly , |
| Relator term | |
| 700 0# - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Maissa Y. Salem , |
| Relator term | |
| 856 ## - ELECTRONIC LOCATION AND ACCESS | |
| Uniform Resource Identifier | <a href="http://172.23.153.220/th.pdf">http://172.23.153.220/th.pdf</a> |
| 905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) | |
| Cataloger | Nazla |
| Reviser | Revisor |
| 905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) | |
| Cataloger | Samia |
| Reviser | Cataloger |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Source of classification or shelving scheme | Dewey Decimal Classification |
| Koha item type | Thesis |
| Source of classification or shelving scheme | Not for loan | Home library | Current library | Date acquired | Full call number | Barcode | Date last seen | Koha item type | Copy number |
|---|---|---|---|---|---|---|---|---|---|
| Dewey Decimal Classification | المكتبة المركزبة الجديدة - جامعة القاهرة | قاعة الرسائل الجامعية - الدور الاول | 11.02.2024 | Cai01.08.03.Ph.D.2018.Ah.A | 01010110075494000 | 22.09.2023 | Thesis | ||
| Dewey Decimal Classification | المكتبة المركزبة الجديدة - جامعة القاهرة | مخـــزن الرســائل الجـــامعية - البدروم | 11.02.2024 | Cai01.08.03.Ph.D.2018.Ah.A | 01020110075494000 | 22.09.2023 | CD - Rom | 75494.CD |