TY - BOOK AU - Rahenda Helmy Mohammad Tammam AU - Eman Yosri Zayed Frag , AU - Gehad Genidy Mohamed , TI - Different analytical methods for the determination of gliclazide drug / PY - 2016/// CY - Cairo : PB - Rahenda Helmy Mohammad Tammam , KW - DDQ KW - Gliclazide KW - TCNQ N1 - Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry; Issued also as CD N2 - This work has been carried out to investigate the: Spectrophotometric determination of gliclazide (GLZ) via charge transfer complex formation with 7, 7, 8, 8-tetracyanoquinodimethane (TCNQ), 2, 3-dichloro-5, 6-dicyano-1, 4-benzoquinone (DDQ) and 2, 5- dichloro-3, 6-dihydroxy-1, 4-benzoquinone (PCA) and estimation of (GLZ) in pure form and pharmaceutical preparations. Structutal investigation of GLZ-DDQ and GLZ-PCA charge transfer complexes using infrared spectroscopy, ultraviolet spectroscopy, mass spectrometry, 1H NMR, X-ray diffraction, element analysis and thermal analysis. Cyclic voltammetric determination of (GLZ) with the utility of both platinum and screen printed electrodes in pure form and pharmaceutical preparations UR - http://172.23.153.220/th.pdf ER -