000 02599cam a2200349 a 4500
003 EG-GiCUC
005 20250223031247.0
008 150708s2014 ua d f m 000 0 eng d
040 _aEG-GiCUC
_beng
_cEG-GiCUC
041 0 _aeng
049 _aDeposite
097 _aPh.D
099 _aCai01.08.03.Ph.D.2014.Da.D
100 0 _aDalia Ahmed Ali Elhaddad
245 1 0 _aDevelopment of analytical methods for the determination of some gastrointestinal tract drugs /
_cDalia Ahmed Ali Elhaddad ; Supervised Badr Edeen A. Elzeany , Samah S. Abbas , Zeinab A. Elsherif
246 1 5 _aاستنباط طرق تحليل لتعيين بعض ادوية الجهاز الهضمى
260 _aCairo :
_bDalia Ahmed Ali Elhaddad ,
_c2014
300 _a231 P. :
_bcharts ;
_c25cm
502 _aThesis (Ph.D.) - Cairo University - Faculty of Pharmacy - Department of Analytical Chemistry
520 _aDifferent methods for the determination of some gastrointestinal drugs including Roxatidine acetate, Tiemonium methylsulphate and Pinaverium bromide were studied. For Roxatidine acetate, stability-indicating TLC-Densitometric, HPLC, ion selective electrode and spectrophotometric D1 methods in the presence of its hydrolytic degradation products have been developed besides establish the degradation pathway by LC-MS. For Tiemonium methylsulphate, stability-indicating TLC-densitometric, HPLC, and spectrophotometric isoabsorptive point, ratio subtraction, D1 and DD1 methods in the presence of its degradation products have been developed besides establish the degradation pathway by LC-MS. For Pinaverium bromide, stability-indicating TLC-densitometric, HPLC and ion selective electrode in the presence of its acid degradation product have been developed besides establish the degradation pathway by LC-MS. All the proposed methods were used for the determination of the cited drugs in bulk powder, pharmaceutical formulations, in presence of their degradation products. The validation was assessed according to ICH guidelines. The obtained results were statistically compared to the manufacturer{u2019}s ones with no significant difference between them
530 _aIssued also as CD
653 4 _aPinaverium bromide
653 4 _aRoxatidine acetate
653 4 _aTiemonium methylsulphate
700 0 _aBadr Eldeen Abdelhalim Elzeany ,
_eSupervisor
700 0 _aSamah Sayed Abbas ,
_eSupervisor
700 0 _aZeinab Abdelaziz Elsherif ,
_eSupervisor
856 _uhttp://172.23.153.220/th.pdf
905 _aEnas
_eCataloger
905 _aNazla
_eRevisor
942 _2ddc
_cTH
999 _c51605
_d51605