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040 _aEG-GiCUC
_beng
_cEG-GiCUC
041 0 _aeng
049 _aDeposite
097 _aPh.D
099 _aCai01.12.11.Ph.D.2019.Mo.E
100 0 _aMohammed Shehata Otiefy Ahmed
245 1 0 _aElectrochemical synthesis of a modified graphite sensor based on nanoparticles /
_cMohammed Shehata Otiefy Ahmed ; Supervised Amany Mohamed Fekry
246 1 5 _aالتصنيع الكهروكيميائى لمجس الجرافيت المعدل المعتمد على الجسيمات النانونية
260 _aCairo :
_bMohammed Shehata Otiefy Ahmed ,
_c2019
300 _a128 P. :
_bcharts , facsimiles ;
_c25cm
502 _aThesis (Ph.D.) - Cairo University - Faculty of Science - Department of Physical Chemistry
520 _aNovel promising electrochemical Caffeine (Caf) sensors were achieved through various ways. Firstly by chemical mixing of Co (II, III) Oxide Nanoparticles on a carbon paste electrode (CPE), secondly by chemical mixing of graphene oxide (GO) nanoparticles and reduced glutathione (GSH) with CP, thirdly by mixing multiwalled carbon nanotubes (MWCNT) and zeolite (Zeo) with CP and/or finally electrodeposition of Ag- nanoparticles on cellulose acetate phthalate (CAP) and chitosan (Chit) polymers with CP. Electrochemical techniques including cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), Chronoamperometry (CA) and differential pulse voltammetry (DPV) were used in the present investigation in addition to analysis techniques like Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), Energy Dispersive X-Ray (EDX) and X-Ray Diffraction (XRD) techniques, in both aqueous and surfactant modified media using sodium dodecyl sulphate (SDS). Caf measurements were investigated in various supporting solutions of pH range (0.75-5.00) containing 0.5 mmol L-1 of SDS. Acceptable results were attained for the finding of Caf in real samples as beverages and drug samples
530 _aIssued also as CD
653 4 _aCaffeine
653 4 _aGORGCPE
653 4 _aNCOMCPE
700 0 _aAmany Mohamed Fekry ,
_eSupervisor
856 _uhttp://172.23.153.220/th.pdf
905 _aAsmaa
_eCataloger
905 _aNazla
_eRevisor
942 _2ddc
_cTH
999 _c75705
_d75705