MARC details
000 -LEADER |
fixed length control field |
02531cam a2200313 a 4500 |
003 - CONTROL NUMBER IDENTIFIER |
control field |
EG-GiCUC |
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
fixed length control field |
190828s2018 ua d f m 000 0 eng d |
040 ## - CATALOGING SOURCE |
Original cataloging agency |
EG-GiCUC |
Language of cataloging |
eng |
Transcribing agency |
EG-GiCUC |
041 0# - LANGUAGE CODE |
Language code of text/sound track or separate title |
eng |
049 ## - LOCAL HOLDINGS (OCLC) |
Holding library |
Deposite |
097 ## - Thesis Degree |
Thesis Level |
M.Sc |
099 ## - LOCAL FREE-TEXT CALL NUMBER (OCLC) |
Classification number |
Cai01.12.08.M.Sc.2018.Mo.P |
100 0# - MAIN ENTRY--PERSONAL NAME |
Personal name |
Mohamed Hamdy Abo Elhamd Ahmed |
245 10 - TITLE STATEMENT |
Title |
Preparation and characterization of modified Ion selective electrodes and their application In determination of some drugs / |
Statement of responsibility, etc. |
Mohamed Hamdy Abo Elhamd Ahmed ; Supervised Mohamed Mohamed Ahmed Omar , Tamer Awad Ali |
246 15 - VARYING FORM OF TITLE |
Title proper/short title |
تحضير و توصيف أقطاب أيونية أنتقائية معدلة و تطبيقاتها فى تقدير بعض الأدوية |
260 ## - PUBLICATION, DISTRIBUTION, ETC. |
Place of publication, distribution, etc. |
Cairo : |
Name of publisher, distributor, etc. |
Mohamed Hamdy Abo Elhamd Ahmed , |
Date of publication, distribution, etc. |
2018 |
300 ## - PHYSICAL DESCRIPTION |
Extent |
112 P. : |
Other physical details |
charts ; |
Dimensions |
25cm |
502 ## - DISSERTATION NOTE |
Dissertation note |
Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry |
520 ## - SUMMARY, ETC. |
Summary, etc. |
The construction and performance characteristics of new modified screen printed (MSPE) and carbon paste (MCPE) electrodes for determination of metoclopramide hydrochloride (MCPHC) drug based on the ion-pair formation between MCP with sodium tetraphenylborate (Na-TPB) in pure, pharmaceutical preparations and biological fluids have been investigated. Different experimental conditions namely types of materials used to fabricate the working electrode (plasticizer), titrant, pH, temperature and life time were studied. The fabricated electrodes demonstrated near Nernstian response over wide linear range of 1.0{u00D7}10{u2013}6-1.0{u00D7}10-2 mol L-1 metoclopramide with lower limit of detection of 1.0{u00D7}10-6 mol L-1 and slopes of 58.10±0.31 mV decade-1 and 58.90±0.15 mV decade-1 over pH range 3.0-8.0 and 3.0{u2013}7.0 for MCPE and MSPE, respectively. The MSPE and MCPE denoted a fast response time of 3 and 2 s and can be utilized at least 83 and 175 days without any remarkable deviations for MCPE and MSPE, respectively. The proposed electrodes displayed good selectivity for MCPHC with respect to number of potential interfering substances as inorganic cations, sugars and other pharmaceutical excipients |
530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE |
Additional physical form available note |
Issued also as CD |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
Metoclopramide hydrochloride |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
Modified carbon paste electrode |
653 #4 - INDEX TERM--UNCONTROLLED |
Uncontrolled term |
Modified screen-printed electrode |
700 0# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Mohamed Mohamed Ahmed Omar , |
Relator term |
|
700 0# - ADDED ENTRY--PERSONAL NAME |
Personal name |
Tamer Awad Ali , |
Relator term |
|
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) |
Cataloger |
Nazla |
Reviser |
Revisor |
905 ## - LOCAL DATA ELEMENT E, LDE (RLIN) |
Cataloger |
Samia |
Reviser |
Cataloger |
942 ## - ADDED ENTRY ELEMENTS (KOHA) |
Source of classification or shelving scheme |
Dewey Decimal Classification |
Koha item type |
Thesis |