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Preparation of different types of ion selective electrodes for determination of econazole nitrate / Hoda Salah Salem Saleh ; Supervised Eman Yossri Zaki , Marwa Elbadry Mohamed

By: Contributor(s): Material type: TextTextLanguage: English Publication details: Cairo : Hoda Salah Salem Saleh , 2015Description: 135 P. : charts ; 25cmOther title:
  • تحضير أنواع مختلفة من الأقطاب الأيونية الإنتقائية لتقذير نتراث الإيكونازول [Added title page title]
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Dissertation note: Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry Summary: In this work, comparative study between MCPE and MSPE modified with different ion pairs as EC-PTA, EC-PMA and EC-RN and the ICPE and ISPE modified with different ion pairing agents as PTA, PMA, RN and NaTPB was described. The electrodes were performed for the determination of econazole nitrate in pure and pharmaceutical forms. The two types of electrodes were characterized and investigated with respect to the experimental parameters affecting their performance including temperature, pH, response time and interference. The electrodes showed good selectivity to ECN with respect to the interfering ions and inorganic cations. Determination of econazole nitrate in pharmaceutical form was performed using calibration, standard addition and potentiometric titration methods. Validation parameters such as accuracy, precision, linearity, specificity, limit of detection and limit of quantification were achieved. The obtained results were in a good agreement with those obtained by the official method
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Item type Current library Home library Call number Copy number Status Date due Barcode
Thesis Thesis قاعة الرسائل الجامعية - الدور الاول المكتبة المركزبة الجديدة - جامعة القاهرة Cai01.12.08.M.Sc.2015.Ho.P (Browse shelf(Opens below)) Not for loan 01010110069127000
CD - Rom CD - Rom مخـــزن الرســائل الجـــامعية - البدروم المكتبة المركزبة الجديدة - جامعة القاهرة Cai01.12.08.M.Sc.2015.Ho.P (Browse shelf(Opens below)) 69127.CD Not for loan 01020110069127000

Thesis (M.Sc.) - Cairo University - Faculty of Science - Department of Analytical Chemistry

In this work, comparative study between MCPE and MSPE modified with different ion pairs as EC-PTA, EC-PMA and EC-RN and the ICPE and ISPE modified with different ion pairing agents as PTA, PMA, RN and NaTPB was described. The electrodes were performed for the determination of econazole nitrate in pure and pharmaceutical forms. The two types of electrodes were characterized and investigated with respect to the experimental parameters affecting their performance including temperature, pH, response time and interference. The electrodes showed good selectivity to ECN with respect to the interfering ions and inorganic cations. Determination of econazole nitrate in pharmaceutical form was performed using calibration, standard addition and potentiometric titration methods. Validation parameters such as accuracy, precision, linearity, specificity, limit of detection and limit of quantification were achieved. The obtained results were in a good agreement with those obtained by the official method

Issued also as CD

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